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SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.高级诊断程序包括全数字化的在线操作手册、维护模拟演示、图片说明等提供快速指导。山东进口分析仪咨询报价
companyprofileShanghaiUzongIndustrialCo.,Ltd.(hereinafterreferredtoasUZONGLAB®)isahigh-techcompanythatprovidesintegratedsolutionsforintelligentlaboratories,mainlyservingtheChinesemarketandcountriesalongthe“BeltandRoad”.IthasthreebusinessdivisionsandoneThetechnologycenter,namelytheinstrumentbusinessdepartment,consumablesbusinessdepartment,projectdevelopmentdepartment,andZhongyuLianheTechnologyCenter.InadditiontotheShanghaiheadquarters,wehaveestablishedbranchesinBeijing,Shenyang,Shijiazhuang,Taiyuan,Qingdao,Guangzhou,ChengduandUrumqi.Toprovidecustomerswithmoreprofessional,saferandmoreconvenientproductsandservicesisoursolegoal.山东进口分析仪咨询报价Cornerstone氧氮氢分析软件同时支持***的数据文档格式和可变的报告格式。
氧氮氢分析仪的常见故障及解决方法:氧和氮空白值超过20。这是由于气流小,不能将炉子中的空气驱赶出去。可调节气体流量,调节载气压力在0.2~0.4MPa。接通仪器载气,放一个石墨坩埚在下电极上,打开主电源开关,点击软件上的关炉按钮,关闭炉子并等待10s。调节流量调节器,直到流量计a显示为30L/h,打开炉子。调节调节器直到流量计b显示为50L/h,再次关闭炉子。如果以上设置不稳定,则增加流量至100L/h,反复调节直至仪器稳定。
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.PlacetheNickelCapsulecontainingthesampleintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.20位试样自动进样系统。
Instrumentcalibration/driftcorrection.a.Loginaminimumof3Standardreplicates.b.Weigha~1.000gramofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.c.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.d.Placethecalibration/driftstandardintotheopenportatthetopoftheloadinghead.e.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.力可**的动态流量补偿控制DFC系统,保证了流量系统的完善,可以精确控制整个气路中的流量。山东进口分析仪咨询报价
可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性,使得分析结果更加准确。山东进口分析仪咨询报价
力可ONH836氧氮氢分析仪特点和优势国际**的非色散红外及热导检测器,无移动部件,不需要手动调整采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测,原理上是**完善的,所以不仅可以保证中间量程的测量精度,在**含量和高含量的检测范围内同样可以满足精度要求高性能的红外检测器配置***恒温绝热技术,消除了外界环境温度的干扰长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性力可的动态流量补偿控制DFC系统,保证了流量系统的完善,可以精确控制整个气路中的流量,保持流量恒定**改善了材料中氮分析的准确度可以旁路的OMI-2气路强化过滤装置增强了检测器的稳定性,使得分析结果更加准确可选自动功能20位试样自动进样系统通用下电极坩埚支座,容纳各种坩埚使用无需人工干预的全自动清扫系统山东进口分析仪咨询报价
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